采用Sol-Gel工艺制备了Si基Bi4Ti3O12铁电薄膜.研究了退火温度对Si基Bi4Ti3O12薄膜晶相结构、晶粒尺寸及薄膜表面形貌的影响.研究表明,退火温度低于450℃时Bi4Ti3O12薄膜为非晶状态,退火温度在550~850℃范围时均为多晶薄膜,而且随退火温度升高,Bi4Ti3O12薄膜更趋向于沿c轴取向的生长;而晶粒尺寸及薄膜粗糙度随退火温度升高而增大,但在较高温度下增长速度趋缓.
Abstract
The ferroelectric thin films of Bi4Ti3O12on Sisubstrates were fabricated by Sol-Gel-technique.The effects of the annealing temperature on crystal phase,grain size and surface morphology of Bi4Ti3O12ferroelectric thin films were studied.The results indicate that the Bi4Ti3O12thin films are amorphous when the annealing temperature is below 450℃,and the Bi4Ti3O12thin films are polycrystalline when the annealing temperatures are from 550℃ to 850℃.Furthermore,the Bi4Ti3O12has a higher degree of texture or prefers orientation in the c axis with the increase of the annealing temperature,the grain size and surface roughness increase with the increase of the anneal-ing temperature as well.
关键词
铁电薄膜 /
Bi4Ti3O12 /
微观结构 /
退火温度
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Key words
ferroelectric thin films /
Bi4Ti3O12 /
microstructures /
annealing temperature
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中图分类号:
TM22.1
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参考文献
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脚注
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基金
国家自然科学基金项目资助(69771024);广西教育厅基金项目资助(桂教科研200156)
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