Please wait a minute...
 
材料工程  2016, Vol. 44 Issue (4): 89-93    DOI: 10.11868/j.issn.1001-4381.2016.04.015
  测试与表征 本期目录 | 过刊浏览 | 高级检索 |
辐照过程中He对ODS合金中氧化物的影响
贺建超1,2, 高进2, 邓东3, 万发荣2
1. 北京航空制造工程研究所, 北京 100024;
2. 北京科技大学 材料科学与工程学院, 北京 100083;
3. 环境保护部 核与辐射安全中心, 北京 100082
Effect of Helium on Oxides in ODS Alloy During Ion Irradiation
HE Jian-chao1,2, GAO Jin2, DENG Dong3, WAN Fa-rong2
1. Beijing Aeronautical Manufacturing Technology Research Institute, Beijing 100024, China;
2. School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China;
3. Nuclear and Radiation Safety Center, Ministry of Environmental Protection, Beijing 100082, China
全文: PDF(3488 KB)   HTML()
输出: BibTeX | EndNote (RIS)      
摘要 研究辐照下He在氧化物弥散强化材料中小于5nm的氧化物颗粒的稳定性。在有He环境下,对14YWT氧化物弥散强化材料进行高温离子辐照。采用三维原子探针(APT)对辐照前后样品中的氧化物颗粒的大小、密度、成分以及其空间分布进行分析。结果表明:小于5nm的弥散氧化物颗粒主要是由Y和Ti的氧化物组成,在辐照前后其成分、尺寸和空间分布无明显变化,说明在600℃高温重离子辐照过程中,在有He环境下铁素体ODS材料中弥散氧化物颗粒仍具有良好的稳定性。
服务
把本文推荐给朋友
加入引用管理器
E-mail Alert
RSS
作者相关文章
贺建超
高进
邓东
万发荣
关键词 氧化物弥散强化材料辐照纳米氧化物颗粒稳定性    
Abstract:The stability of nano-scale oxides with the size less than 5nm in the helium atmosphere under irradiation in the ODS(oxide dispersion strengthened) materials was researched. The 14YWT alloy with pre-implanted with helium was irradiated at high temperature. Size, density, and composition of the nano-scale oxides were investigated by the atom probe tomography. The results show that nano-scale oxides are composed of oxides enrich in Ti and Y. The change of the size and composition of the nano-scale oxides under irradiation is trivial, indicating the good stability of nano-scale oxides in helium pre-implanted ODS materials under irradiation at 600℃.
Key wordsODS material    irradiation    nano-scale oxide particle    stability
收稿日期: 2014-02-17      出版日期: 2016-04-19
中图分类号:  TL67  
通讯作者: 万发荣(1955-),男,教授,从事核聚变堆结构材料的辐照损伤的研究工作,联系地址:北京科技大学材料科学与工程学院(100083)     E-mail: wanfr@mater.ustb.edu.cn
引用本文:   
贺建超, 高进, 邓东, 万发荣. 辐照过程中He对ODS合金中氧化物的影响[J]. 材料工程, 2016, 44(4): 89-93.
HE Jian-chao, GAO Jin, DENG Dong, WAN Fa-rong. Effect of Helium on Oxides in ODS Alloy During Ion Irradiation. Journal of Materials Engineering, 2016, 44(4): 89-93.
链接本文:  
http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2016.04.015      或      http://jme.biam.ac.cn/CN/Y2016/V44/I4/89
[1] ZINKLE S J, WAS G S. Materials challenges in nuclear energy[J]. Acta Materials,2013,61(3):735-758.
[2] ODETTE G R, ALINGER M J, WIRTH B D,et al. Recent developments in irradiation resistant steels[J]. Annual Review of Materials Research,2008,38:471-503.
[3] 吕铮,刘春明. 抗辐照合金的发展与纳米结构ODS钢的抗辐照性能[J].材料与冶金学报,2012,11(1):48-52. LU Z, LIU C M. Development of radiation-resistant alloys and radiation tolerance of nano-structured ODS steels[J]. Journal of Materials and Metallurgy,2012,11(1):48-52.
[4] 李明,周张健,廖璐,等. ODS铁素体钢中弥散氧化物的研究进展[J].材料导报:综述篇,2010,24(8):94-98. LI M, ZHOU Z J, LIAO L,et al. Research progress of dispersed oxides in ODS ferritic steels[J].Materials Review,2010,24(8):94-98.
[5] UKAI S, FUJIWARA M. Perspective of ODS alloys application in nuclear environments[J].Journal of Nuclear Materials,2002,307(1):749-757.
[6] WU Y, HANEY E M, CUNNINGHAM N J, et al. Transmission electron microscopy characterization of the nanofeatures in nanostructured ferritic alloy MA957[J].Acta Materialia,2012,60(8):3456-3468.
[7] KLUEHR L,SHIGLEDECKER J P, SWINDEMAN R W, et al. Oxide dispersion-strengthened steels:a comparison of some commercial and experimental alloys[J]. Journal of Nuclear Materials,2005,341(2-3):103-114.
[8] WILLIAMS C A, UNIFANTOWICZ P, BALUC N, et al. The formation and evolution of oxide particles in oxide-dispersion-strengthened ferritic steels during processing[J]. Acta Materialia,2013,61(6):2219-2235.
[9] HSIUNGL L, FLUSS M J, KIMURA A. Structure of oxide nanoparticles in Fe-16Cr MA/ODS ferritic steel[J]. Materials Letters,2010,64(16):1782-1785.
[10] PARISHC M, EDMONDSON P D, ZHANG Y. Direct observation of ion-irradiation-induced chemical mixing[J]. Journal of Nuclear Materials,2011,418(1-3):106-109.
[11] LESCOATA M L, RIBISA J, GENTILS B. In situ TEM study of the stability of nano-oxides in ODS steels under ion-irradiation[J]. Journal of Nuclear Materials,2012,428(1-3):176-182.
[12] KIM I S, HUNN J D, HASHIMOTO N. Defect and void evolution in oxide dispersion strengthened ferritic steels under 3.2MeV Fe ion irradiation with simultaneous helium injection[J]. Journal of Nuclear Materials,2000,280(3):264-274.
[13] 胡本芙, 郭丽娜, 贾成厂,等.双束(He+/e-)辐照下氦对12Cr-ODS铁素体钢组织损伤影响研究[J].核动力工程,2011,32(3):48-51. HU B F, GUO L N, JIA C C,et al. Effect of He on 12Cr-ODS ferritic steel structural damage during(He++e-) dual-beam irradiation[J]. Nuclear Power Engineering, 2011,32(3):48-51.
[14] HOELZER D T, BENTLEY J, SOKOLOV M A.Influence of particle dispersions on the high-temperature strength of ferritic alloys[J]. Journal of Nuclear Materials,2007,367:166-172.
[15] STOLLER R E, TOLOCZKO M B, WAS G S,et al.On the use of SRIM for computing radiation damage exposure[J].Nuclear Instruments and Methods in Physics Research Section B,2013,310(11):75-80.
[16] MILLER M K. Atom Probe Tomography[M]. New York:Springer,2000.
[17] HYDE J M,MARQUIS E A, WILFORD K B,et al. A sensitivity analysis of the maximum separation method for the characterization of solute clusters[J]. Ultramicroscopy,2011,111(6):440-447.
[18] MILLERMK,RUSSELL K F, HOELZER D T,et al. Characterization of precipitates in MA/ODS ferritic alloys[J]. Journal of Nuclear Materials,2006,351(1-5):261-268.
[19] MILLER M K,KENIK E A, RUSSELL K F,et al. Atom probe tomography of nanoscale particles in ODS ferritic alloys[J]. Materials Science and Engineering:A,2003,353(1-2):140-145.
[20] ALINGER M J,ODETTEG R, HOELZER D T,et al. On the role of alloy composition and processing parameters in nanocluster formation and dispersion strengthening in nanostuctured ferritic alloys[J]. Acta Materialia,2009,57(2):392-406.
[21] MILLER M K, HOELZER D T,KENIK E A,et al. Nanometer scale precipitation in ferritic MA/ODS alloy MA957[J]. Journal of Nuclear Materials,2004,329-333(8):338-341.
[22] MARQUIS E A. Core/shell structures of oxygen-rich nanofeatures in oxide-dispersion strengthened FeCr alloys[J]. Applied Physics Letters,2008,93(18):1904-1906.
[23] HIRATA A, FUJITA T, WEN Y R,et al. Atomic structure of nanoclusters in oxide-dispersion-strengthened steels[J]. Nature Materials,2011,10(12):923-926.
[24] KLIMENKOV M,LINDAUR, MÖSLANG A,et al. New insights into the structure of ODS particles in the ODS-Euroferalloy[J]. Journal of Nuclear Materials,2009,386-388:553-556.
[25] De CASTRO V, LOZANO P S, JENKINS M L. Stability of nanoparticles in an oxide dispersion strengthened alloy[J].Journal of Physics:Conference Series,2010,241(1):1-7.
[26] KISHIMOTO H, KASADA R, HASHITOMI O. Stability of Y-Ti complex oxides in Fe-16Cr-0.1Ti ODS ferritic steel before and after heavy-ion irradiation[J]. Journal of Nuclear Materials,2009,386-388:533-536.
[27] ROBERTSON C, PANIGRAHI B K, BALAJI S.Particle stability in model ODS steel irradiated up to 100dpa at 600℃:TEM and nano-indentation investigation[J].Journal of Nuclear Materials,2012,426(1-3):240-246.
[28] ALLEN T R, GAN J, COLE J I, et al.Radiation response of a 9 chromium oxide dispersion strengthened steel to heavy ion irradiation[J]. Journal of Nuclear Materials,2008,375(1):26-37.
[29] LIU C, YU C, HASHIMOTO N.Micro-structure and micro-hardness of ODS steels after ion irradiation[J].Journal of Nuclear Materials,2011,417(1-3):270-273.
[30] CERTAIN A, KUCHIBHATLA S, SHUTTHANANDAN V. Radiation stability of nanoclusters in nano-structured oxide dispersion strengthened(ODS) steels[J]. Journal of Nuclear Materials,2013,434(1-3):311-321.
[1] 李亚锋, 礼嵩明, 黑艳伟, 邢丽英, 陈祥宝. 太阳辐照对芳纶纤维及其复合材料性能的影响[J]. 材料工程, 2019, 47(4): 39-46.
[2] 胡安俊, 龙剑平, 舒朝著. 设计稳定和可逆的锂-空气电池阴极催化剂的研究进展[J]. 材料工程, 2019, 47(3): 30-41.
[3] 董雪, 马爽, 武晓霞, 那日苏. Fe52T2(T=Cr,Mn,Co,Ni)合金bcc与fcc相结构的第一性原理研究[J]. 材料工程, 2019, 47(3): 147-153.
[4] 周堃, 刘杰, 赵宇. 硅橡胶密封件长期贮存老化行为[J]. 材料工程, 2018, 46(8): 163-168.
[5] 何培, 姚伟志, 吕建明, 张向东. 聚变堆结构材料辐照性能的评价[J]. 材料工程, 2018, 46(6): 19-26.
[6] 李晓敏, 吴菊英, 唐昶宇, 袁萍, 邢涛, 张凯, 梅军, 黄渝鸿. B4CP/PI聚酰亚胺复合薄膜耐高温及热中子辐照屏蔽性能研究[J]. 材料工程, 2018, 46(3): 48-54.
[7] 朱文华, 岳建岭, 黄小忠, 王春齐, 胡思闽, 王畅. 电子束辐照含铍聚碳硅烷制备含铍碳化硅纤维[J]. 材料工程, 2018, 46(12): 54-60.
[8] 李可峰, 尹晓燕. 聚苯醚纳米纤维锂电隔膜的制备[J]. 材料工程, 2018, 46(10): 120-126.
[9] 李春燕, 尹金锋, 王铮, 寇生中, 赵燕春. Er对ZrCuNiAl非晶合金结构、力学性能、热稳定性及非晶形成能力的影响[J]. 材料工程, 2018, 46(1): 1-7.
[10] 李娜, 马兆昆, 陈铭, 宋怀河, 李昂, 贾月荣. 石墨烯/聚酰亚胺复合石墨纤维的结构与性能[J]. 材料工程, 2017, 45(9): 31-37.
[11] 郑顺丽, 李澄, 项腾飞, 胡玮, 丁诗炳, 王晶, 刘盼金. 阳极氧化法制备铝基超疏水涂层及其稳定性和耐蚀性的研究[J]. 材料工程, 2017, 45(10): 71-78.
[12] 桑伟, 周岚, 冯新星, 张建春. 电子束辐照诱导丙烯酸接枝尼龙66织物的改性研究[J]. 材料工程, 2017, 45(10): 111-116.
[13] 党莹樱, 赵新宝, 尹宏飞, 鲁金涛, 袁勇, 杨珍, 谷月峰. Inconel 740H合金750℃长期时效后的组织稳定性[J]. 材料工程, 2016, 44(9): 58-62.
[14] 万响亮, 李光强, 周博文, 马江华. 奥氏体不锈钢晶粒细化对形变机制和力学性能的影响[J]. 材料工程, 2016, 44(8): 29-33.
[15] 刘晓丽, 鹿海军, 邢丽英. 发泡剂含量对双马来酰亚胺泡沫泡孔结构和性能的影响[J]. 材料工程, 2016, 44(5): 42-46.
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed   
版权所有 © 2015《材料工程》编辑部
地址:北京81信箱44分箱 邮政编码: 100095
电话:010-62496276 E-mail:matereng@biam.ac.cn
本系统由北京玛格泰克科技发展有限公司设计开发 技术支持:support@magtech.com.cn