In order to solve the forming difficulty of the ceramic matrix composites used as the aeroengine complex components, carbon fiber fabric was used as the reinforcement, two different slurries, with or without powder additives, were taken to form the carbon fiber fabric reinforced silicon carbide composites via slurry-casting and melt infiltration technology. The process adaptability of the two slurries in the slurry-casting and melt infiltration process were explored, and corresponding basic properties of the composites were investigated. The results show that the viscosity of the two slurries is moderate during the slurry-casting process, and they could keep the station for more than 3-5 hours at the setting temperatures, which could obtain dense and uniform polymer matrix composites. After being carbonized at 900 ℃, the porosity of the solidified sample synthesized via slurries with or without powder is 39.6% and 31.3%, the residual carbon ratio is 24% and 76%, and the average diameter of pore is 0.068 μm and 0.069 μm, respectively. The carbon fiber fabric-reinforced silicon carbide composite prepared with powder-added slurry has lower porosity of 3.54% and higher bending strength of 162 MPa, which meets the application requirements of aeroengine static components.
ZHANG L T , CHENG L F . Discussion on strategies of sustainable development of continuous fiber reinforced ceramic matrix composites[J]. Acta Materiae Compositae Sinica, 2007, 24 (2): 1- 6.
doi: 10.3321/j.issn:1000-3851.2007.02.001
HE X B , YANG H , ZHANG C R , et al. Review of continuous fiber reinforced ceramic matrix composites[J]. Materials Science and Engineering, 2002, 20 (2): 273- 278.
doi: 10.3969/j.issn.1673-2812.2002.02.034
LIU D X . One generation of new material, one generation of new type engine: development trend of aero-engine and its requirements for materials[J]. Journal of Materials Engineering, 2017, 45 (10): 1- 5.
doi: 10.11868/j.issn.1001-4381.2017.100001
ZHANG Y D , ZHOU X G , ZHANG C R . Development and application of Cf/SiC ceramic matrix composites[J]. Journal of Materials Engineering, 2005, (4): 60- 63.
doi: 10.3969/j.issn.1001-4381.2005.04.015
5
IMUTA M , GOTOH J . Development of high temperature materials including CMCs for space application[J]. Key Engineering Material, 1999, 164/165, 439- 444.
LIU Q M , HUANG S Z , HE A J . Application requirements and challenges of CMC-SiC composites on aero-engine[J]. Journal of Materials Engineering, 2019, 47 (2): 1- 10.
doi: 10.3969/j.issn.1673-1433.2019.02.001
JIAO J , LIU S H . Progress in ceramic matrix composites fabricated by chemical by chemical vapor infiltration[J]. Aeronautical Manufacturing Technology, 2015, (14): 101- 104.
8
BLAGOEVA D T , HEGEMAN J B J , JONG M , et al. Characterisation of 2D and 3D Tyranno SA3 CVI SiCf/SiC composites[J]. Materials Science and Engineering: A, 2015, 638, 305- 313.
doi: 10.1016/j.msea.2015.04.090
9
BERTRAND D J , SABELKIN V , ZAWADA L , et al. Fatigue behavior of Sylramic-iBN/BN/CVI SiC ceramic matrix composite in combustion environment[J]. Journal of Materials Science, 2015, 50, 7437- 7447.
doi: 10.1007/s10853-015-9302-8
FENG Q , WANG W Q , WANG Z , et al. Microstructure analysis of SiC matrix composites reinforced by carbon fibers and SiC fibers[J]. Research and Exploration in Laboratory, 2010, 29 (1): 44- 46.
doi: 10.3969/j.issn.1006-7167.2010.01.016
WANG Y F , LIU W F , MA Q S . Effects on the thermal conductivity properties of SiCf/SiC composites manufactured by PIP process[J]. Rare Metal Materials and Engineering, 2009, 38 (2): 466- 469.
12
ENRICO K , ALEXANDER F , MARTIN F , et al. Mechanical and microstructural characterisation of SiC- and SiBNC-fibre reinforced CMCs manufactured via PIP method before and after exposure to air[J]. Journal of the European Ceramic Society, 2012, 32 (14): 3861- 3874.
doi: 10.1016/j.jeurceramsoc.2012.05.028
13
LUO Z , CAO H , REN H , et al. Tension-tension fatigue behavior of a PIP SiC/SiC composite at elevated temperature in air[J]. Ceramics International, 2016, 42 (2): 3250- 3260.
doi: 10.1016/j.ceramint.2015.10.116
JIAO J , YANG J H , LI B W . Progress in ceramic matrix composites fabricated by melt infiltration progress[J]. Aeronautical Manufacturing Technology, 2015, (Suppl 2): 1- 6.
DONG S M , HU J B , ZHANG X Y . Melt infiltration process for SiC/SiC composites[J]. Aeronautical Manufacturing Technology, 2014, (6): 35- 40.
doi: 10.3969/j.issn.1671-833X.2014.06.005
16
BRENNAN J J . Interfacial characterization of a slurry-cast melt-infiltrated SiC/SiC ceramic-matrix composite[J]. Acta Materialia, 2000, 48 (18/19): 4619- 4628.
ZHANG X L , LV Z L , JIN Z H . Influence factor of MoSi2-SiC composites synthesised by reactive infiltration[J]. Rare Metal Materials and Engineering, 2005, 34 (4): 639- 642.
doi: 10.3321/j.issn:1002-185X.2005.04.031
18
NAROTTAM P B . Handbook of ceramic composites[M]. London: Kluwer Academic Publishers, 2005: 100- 103.
LIU H , YANG J H , CHEN Z M , et al. Microstructure and properties of SiCf/SiC composite fabricated by melt infiltration process[J]. Aerospace Materials & Technology, 2020, 50 (6): 48- 54.