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2222材料工程  2022, Vol. 50 Issue (2): 1-11    DOI: 10.11868/j.issn.1001-4381.2021.000295
  生物医用材料专栏 本期目录 | 过刊浏览 | 高级检索 |
牙科陶瓷材料的摩擦学性能研究进展
雷磊1, 伍雨驰1, 程子晋1, 刘莉2, 郑靖1,*()
1 西南交通大学 材料先进技术教育部重点实验室 摩擦学研究所, 成都 610031
2 西南交通大学医院 口腔科, 成都 610031
Research progress in tribological property of dental ceramics
Lei LEI1, Yuchi WU1, Zijin CHENG1, Li LIU2, Jing ZHENG1,*()
1 Tribology Research Institute, Key Laboratory of Advanced Technologies of Materials(Ministry of Education), Southwest Jiaotong University, Chengdu 610031, China
2 Department of Stomatology, Southwest Jiaotong University Hospital, Chengdu 610031, China
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摘要 

陶瓷材料因其优异的耐磨性、化学稳定性、生物相容性和美观性被广泛用于牙齿缺损和缺失修复。本文首先介绍了牙科陶瓷材料的化学成分、微观结构和力学性能，基于陶瓷材料的磨损与磨蚀机制，归纳总结了牙科陶瓷材料摩擦学性能优化方面所取得的进展，指出陶瓷材料和天然人牙摩擦学性能失配严重制约了陶瓷修复体的临床应用，进而从室验介质、对摩副以及载荷、位移和循环次数等方面分析汇总牙科陶瓷材料摩擦学性能的体外测试方法。最后，从仿生摩擦学角度探讨了牙科陶瓷材料的未来发展趋势，并指出研制仿生陶瓷基复合材料是解决陶瓷修复体与天然人牙摩擦学性能失配难题最具潜力的策略。
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雷磊
伍雨驰
程子晋
刘莉
郑靖
关键词 ： 牙科陶瓷材料,  摩擦学性能,  测试方法,  微观结构,  仿生设计    
Abstract：

Ceramics are widely used as dental restorative materials because of their superior wear resistance, chemical stability, biocompatibility, and aesthetic features. In this paper, the chemical compositions, microstructures and mechanical properties of dental ceramics were introduced, based on the wear mechanisms of typical dental ceramics and their abrasiveness with opposing human teeth, the main progress concerning the tribological performance optimization of dental ceramics were summarized, and it was pointed out that the mismatch of tribological properties between ceramics and human teeth seriously restricts the clinical application of dental ceramics. Then the in vitro test methods of tribological properties of dental ceramic materials are analyzed and summarized from the aspects of laboratory test medium, friction pair, load, displacement and cycle times. Finally, the future development trends of dental ceramics were discussed from the perspective of bionic tribology. It was pointed out that bionic design of ceramic matrix composites is a promising strategy for overcoming the mismatch of tribological property between dental ceramic restorations and human teeth.
Key words： dental ceramics    tribological property    test method    microstructure    bioinspired design
收稿日期: 2021-04-01      出版日期: 2022-02-23
中图分类号:  R318.08  
基金资助:国家自然科学基金资助项目(52035001);国家自然科学基金资助项目(51535010);高等学校学科创新引智计划资助项目(B20008)
通讯作者: 郑靖     E-mail: jzheng168@home.swjtu.edu.cn
作者简介: 郑靖(1974-), 女, 研究员, 博士, 研究方向: 生物与仿生摩擦学, 联系地址: 四川省成都市西南交通大学摩擦学研究所(610031), E-mail: jzheng168@home.swjtu.edu.cn
引用本文:   
雷磊, 伍雨驰, 程子晋, 刘莉, 郑靖. 牙科陶瓷材料的摩擦学性能研究进展[J]. 材料工程, 2022, 50(2): 1-11.
Lei LEI, Yuchi WU, Zijin CHENG, Li LIU, Jing ZHENG. Research progress in tribological property of dental ceramics. Journal of Materials Engineering, 2022, 50(2): 1-11.
链接本文:  
http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2021.000295      或      http://jme.biam.ac.cn/CN/Y2022/V50/I2/1
Material Composition Characteristic Mechanical property Reference
Feldspathic porcelains Mainly glass phase and a few crystal phase comprising leucite Good aesthetics but poor mechanical performance E=45-60 GPa;
H=3.6-6.0 GPa;
σ=64-104 MPa;
KIC=0.7-1.2 MPa·m1/2		 [5, 18-23]
Glass-ceramics Crystal phase comprising leucite, lithium disilicate, mica and fluorapatite and glass phase High crystal content, increased mechanical performance, but decreased translucency E=65-105 GPa;
H=3.4-8.4 GPa;
σ=110-400 MPa;
KIC=1.1-3.0 MPa·m1/2		 [5, 24-29]
Glass-infiltrated ceramics Crystal phase comprising alumina, spinel and zirconia and glass phase Good mechanical performance, some types have poor translucency E=166-300 GPa;
H=7.4-12.9 GPa;
σ=233-600 MPa;
KIC=3.1-4.6 MPa·m1/2		 [30-33]
Polycrystalline ceramics Crystal phase comprising alumina, zirconia, etc Excellent mechanical performance E=200-240 GPa;
H=12-13 GPa;
σ=680-1200 MPa;
KIC=3.5-10.0 MPa·m1/2		 [29, 34-40]
Polymer infiltrated ceramics Feldspathic porcelain and methacrylate resin Human tooth-matching elasticity modulus and hardness E=16.4-38.4 GPa;
H=1.1-3.4 GPa;
σ=124-281 MPa;
KIC=1.0-1.7 MPa·m1/2		 [41-47]
Table 1  牙科陶瓷材料分类[5, 18-47]
Group Wear mechanism Abrasive potential Reference
Feldspathic porcelains Fatigue wear and brittle delamination initially occur in glass phase matrix and then lead to overall abrasive wear High abrasive potential, generally causing strong plough effect on the surface of opposing human enamel [48-50]
Glass-ceramics Crystal-glass interface cracking results in ceramic particle exfoliation and abrasive wear Hard crystal particles cause severe abrasive wear on opposing human enamel surface [51-54]
Glass-infiltrated ceramics (glass-infiltrated alumina ceramics) Tribochemical reaction induces the formation of wear debris layer with anti-wear effect, leading to excellent wear-resistance No clear report on their abrasive potential to human enamel [55-57]
Polycrystalline ceramics (zirconia ceramics) High strength and toughness can effectively resist surface damage, leading to excellent wear-resistance Low abrasive potential, and the wear mechanism of opposing human enamel is fatigue wear [39, 58]
Polymer infiltrated ceramics The wear of polymer phase causes ceramic framework protruding and ceramic particles exfoliation, causing weak wear-resistance Low abrasive potential due to human tooth-matching elasticity modulus and hardness [59-60]
Table 2  牙科陶瓷材料的磨损机制与磨蚀性[39, 48-60]
Fig.1  牙科陶瓷材料磨损表面扫描电镜形貌
(a)长石质瓷[50]；(b)玻璃陶瓷[51]；(c)玻璃渗透氧化铝陶瓷[56]
Fig.2  氧化锆陶瓷磨损表面SEM形貌[39]
(a)磨损表面的犁沟；(b)图(a)中心区域的放大图
Fig.3  树脂渗透陶瓷表面SEM形貌[59]
(a)原始表面；(b)磨损初期；(c)稳定磨损阶段
Fig.4  人牙釉质磨损表面SEM形貌
(a)与长石质瓷对摩[58]；(b)与氧化锆陶瓷抛光表面对摩[58]；(c)与树脂渗透陶瓷对摩[60]
Fig.5  摩擦磨损试验机示意图 (a)往复式；(b)销盘式
Fig.6  人牙釉质跨尺度多级结构示意图[89]
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