内生非晶复合材料组织与力学性能调控研究进展

doi:10.11868/j.issn.1001-4381.2021.000328

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摘要

非晶合金因其独特的短程有序、长程无序原子结构特征, 使其具有了一系列优异的力学、物理、化学等性能, 在先进金属结构材料领域具有巨大的潜在应用价值。但非晶合金在室温承载变形时, 原子团簇发生剪切转变形成的大量自由体积会演化为高度局域化剪切带, 局域化剪切带由于缺乏介质的阻碍会发生失稳扩展, 导致非晶合金极易发生室温脆断, 特别单轴拉伸时基本无塑性。为克服这个缺憾, 研究者们提出将微米级尺寸的晶体相引入非晶来抑制剪切带的失稳扩展, 使得内生第二相增韧非晶复合材料具有了明显的拉伸塑性能力, 因此倍受材料学界的关注。近年来, 研究者们陆续通过成分设计、制备技术、热处理工艺等方法来实现非晶复合材料的塑性变形能力的提升, 使得非晶复合材料有望走向实际的工程应用。本文围绕内生第二相增韧非晶复合材料的微观组织调控这一关键科学问题, 从影响非晶复合材料微观组织结构的因素(合金成分设计、制备工艺参数、微观结构构筑等)到微观组织对其室温力学性能的影响机制两方面的研究成果进行了系统总结, 重点阐述了近10年来内生第二相增韧非晶复合材料领域组织调控及其室温力学性能关联性方面的研究进展, 并且对内生非晶复合材料研究领域目前的存在的问题和挑战进行了展望, 以期为高强高韧内生第二相增韧非晶复合材料的设计与制备提供理论参考。

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	翟海民
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	欧梦静
	李文生

关键词 ：非晶复合材料, 微观组织调控, 制备技术, 力学性能, 剪切带

Abstract：

Metallic glasses (MGs) have a series of excellent mechanical, physical, chemical and other properties due to their unique short-range ordered and long-range disordered atomic structure characteristics, making them have great potential application value in the field of advanced metal structural materials. However, when the bulk metallic glass (BMG) is deformed under room temperature, the large amount of free volume formed by the shear transformation of the atomic clusters will evolve into a highly localized shear bands. The localized shear bands will undergo instability expansion due to the lack of media, which leads to the fact that BMGs are very prone to brittle fracture at room temperature. In particular, there is no plasticity during uniaxial tension. In order to overcome this shortcoming, the researchers proposed to introduce the micron-sized crystal phase into the glass matrix to suppress the instability expansion of the shear band, so that the in-situ dendritic toughened bulk metallic glass composite (BMGC) has obvious tensile plasticity, and the BMGC has attracted much attention from the material science community. In recent years, researchers have successively improved the plastic deformation ability of BMGC through composition design, preparation technology, heat treatment process and other methods, making BMGC be expected to move towards practical engineering applications. This article focuses on the key scientific issue of microstructure control of in-situ second-phase toughened BMGC, from the factors that affect the microstructure of BMGC (alloy composition design, preparation process parameters, microstructure construction, etc.) to the mechanism of the influence of microstructure on its room temperature mechanical properties, the research results were systematically summarized. In particular, the article focuses on the research progress in the field of in-situ second-phase toughened BMGC in the past 10 years in the field of microstructure regulation and the correlation between mechanical properties at room temperature. In addition, the current problems and challenges in the field of in-situ second-phase toughened BMGC were addressed. The prospects are expected to provide a theoretical reference for the design and preparation of high-strength and high-toughness in-situ second-phase toughened BMGC.

Key words： bulk metallic glass composites microstructure regulation preparative technique mechanical property shear band

收稿日期: 2021-04-09 出版日期: 2022-05-23

中图分类号:

TG146.4

基金资助:国家自然科学基金项目(51901092);国家自然科学基金项目(52075234);科技部丝绸之路经济带金属表面工程技术国家国际科技合作基地项目(2017D01003);甘肃省青年科技基金计划(20 JR5RA431);兰州理工大学红柳优秀青年人才支持计划(26/062005);湖南理工学院湖南省电磁装备设计与制造重点实验室开放基金资助课题(DC202001)

通讯作者: 翟海民,李文生 E-mail: hmzhai@lut.edu.cn;liws@lut.edu.cn

作者简介: 李文生(1973—)，男，教授，博士，主要从事金属表面防护与延寿技术领域研究及工程化应用工作，联系地址：甘肃省兰州市七里河区兰工坪路287号兰州理工大学材料科学与工程学院(730050)，E-mail: liws@lut.edu.cn
翟海民(1988—)，男，副研究员，博士，主要从事非晶复合材料及非晶涂层的强韧化机制研究，联系地址：甘肃省兰州市七里河区兰工坪路287号兰州理工大学省部共建有色金属先进加工与再利用国家重点实验室(730050)，E-mail: hmzhai@lut.edu.cn

引用本文:

翟海民, 马旭, 袁花妍, 欧梦静, 李文生. 内生非晶复合材料组织与力学性能调控研究进展[J]. 材料工程, 2022, 50(5): 78-89.
Haimin ZHAI, Xu MA, Huayan YUAN, Mengjing OU, Wensheng LI. Research progress in control of microstructure and mechanical properties of in-situ bulk metallic glass composites. Journal of Materials Engineering, 2022, 50(5): 78-89.

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http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2021.000328 或 http://jme.biam.ac.cn/CN/Y2022/V50/I5/78

Fig.1 Zr-(Ti+Nb)-(Cu₅Ni₄Be₉)伪三元相图^[38]

Fig.2 (Zr₇₅Ti₁₅Nb₁₀)_100-y(Be₅₀Cu_27.5Ni_22.5)_y BMGCs随y值变化的组织演变图^[41]
(a)y=32, V_d=8%;(b)y=30, V_d=21%；(c)y=29, V_d=25%；(d)y=27；V_d=32%；(e)y=26, V_d=38%；(f)y=20, V_d=55%

Fig.3 梯度DH3 BMGC的拉伸变形行为^[23]
(a)拉伸工程应力-应变曲线;(b)梯度BMGC的拉伸断裂形貌;(c)第5层和第6层之间界面处的典型扩大区域

Fig.4 Ti_47-xZr₂₅Nb₆Cu₅Be₁₇Sn_x (x=0%, 1%, 2%, 3%, 4%) BMGCs的枝晶和非晶杨氏模量随Sn含量变化(a)及不同Sn含量BMGCs拉伸工程应力-应变曲线(b)^[31]

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