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2222材料工程  2021, Vol. 49 Issue (5): 48-55    DOI: 10.11868/j.issn.1001-4381.2020.000416
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水滑石作为润滑油(脂)添加剂的摩擦性能及其影响因素
李桂金1,2, 张忠伦1,2, 白志民3,*()
1 中建材科创新技术研究院(山东)有限公司, 山东 枣庄 277100
2 中国建筑材料科学研究总院有限公司, 北京 100024
3 中国地质大学(北京) 材料科学与工程学院, 北京 100083
Friction performance of hydrotalcite as lubrication oil (grease) additive and its influence factors
Gui-jin LI1,2, Zhong-lun ZHANG1,2, Zhi-min BAI3,*()
1 CNBM Technology Innovation Academy (shandong) Co., Ltd., Zaozhuang 277100, Shandong, China
2 China Building Materials Academy Co., Ltd., Beijing 100024, China
3 School of Materials Science and Technology, China University of Geoscience(Beijing), Beijing 100083, China
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摘要 

水滑石应用于机械摩擦系统，展现出良好的减摩抗磨性能。本文系统总结水滑石作为润滑油（脂）添加剂的摩擦性能及其影响因素，重点分析制备方法、阳离子半径、二价与三价阳离子比例、层间无机阴离子种类、有机阴离子插层、结晶度等因素对水滑石减摩抗磨性能的影响规律与作用机制，明确水滑石润滑材料结构成分设计基本原则与调控方向。基于研究现状，提出应深入加强水滑石润滑材料工业实验验证、水滑石对润滑油（脂）品质影响评价、水滑石与摩擦副表面交互作用基础研究等工作。
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李桂金
张忠伦
白志民
关键词 ： 水滑石,  减摩抗磨,  影响因素,  研究方向    
Abstract：

Hydrotalcite applied in mechanical friction system exhibits good friction and wear resistance. Friction performance of hydrotalcite as lubrication oil (grease) additive and its influence factors were summarized systematically in this paper. The mechanism and regulation of preparation methods, cation radius, the ratio of divalent and trivalent cations, the type of inorganic anions between layers, the intercalation of organic anions, crystallinity on the friction reduction and antiwear properties were analyzed comparatively. The basic principle and control directions of the structural composition design of hydrotalcite lubrication materials were clarified. Based on the research status, it was suggested that the industrial test verification of hydrotalcite, the evaluation of the influence of hydrotalcite on the quality of lubricating oil (grease), and the basic research about the interaction between hydrotalcite and the friction surface should be strengthened.
Key words： hydrotalcite    friction reduction and antiwear    influence factor    research direction
收稿日期: 2020-05-08      出版日期: 2021-05-21
中图分类号:  P578.964  
基金资助:国家重点研发计划项目(2017YFB0310700)
通讯作者: 白志民     E-mail: zhimibai@cugb.edu.cn
作者简介: 白志民(1957-), 男, 教授, 博士, 研究方向为工业矿物与岩石材料的综合利用, 联系地址: 北京市海淀区学院路29号中国地质大学(北京)材料科学与工程学院(100083), zhimibai@cugb.edu.cn
引用本文:   
李桂金, 张忠伦, 白志民. 水滑石作为润滑油(脂)添加剂的摩擦性能及其影响因素[J]. 材料工程, 2021, 49(5): 48-55.
Gui-jin LI, Zhong-lun ZHANG, Zhi-min BAI. Friction performance of hydrotalcite as lubrication oil (grease) additive and its influence factors. Journal of Materials Engineering, 2021, 49(5): 48-55.
链接本文:  
http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2020.000416      或      http://jme.biam.ac.cn/CN/Y2021/V49/I5/48
Ion Coordination Spin state Ionic radius/10-1 nm
Zn2+ 6 0.74
Co2+ 6 LS; HS 0.65;0.745
Co3+ 6 LS; HS 0.545;0.61
Ni2+ 6 HS 0.69
Mg2+ 6 0.72
Cu2+ 6 0.73
Al3+ 6 0.535
Ce3+ 6 1.01
La3+ 6 1.032
Table 1  阳离子半径[42]
Experimental condition LDH FCD*/% API*/% Reference
Four ball test，rotary speed 1200 r/min，load 392 N, run time
30 min，dosage 10 g/L		 Co-Al-CO3 49.1 33.1 [39]
Four ball test，rotary speed 1200 r/min, load 392 N，run time
60 min, dosage 5 g/L		 Mg-Al-NO3
Ni-Al-NO3
Co-Al-CO3		 12.9
17.3
22.3		 5.0
14.7
26.1		 [36]
Gear experiment, load 45 N, rotary speed 2800 r/min, run time 10 h, dosage 10 g/L Ni-Mg-Al-CO3
Cu-Mg-Al-CO3		 10.6
8
Air compressor experiment, after the air pressure rises to 20 kPa, run time 30 min, dosage 10 g/L Ni-Mg-Al-CO3
Cu-Mg-Al-CO3		 4.1
3.8		 [44]
Pin disc test, speed 0.5 m/s, load 10 N, run distance 450 m, dosage 0.5%(mass fraction) Mg-Al-CO3
Zn-Al-CO3
Zn/Mg-Al-CO3		 39
26
18		 59
29
6		 [45]
Table 2  不同二价阳离子水滑石减摩抗磨性能
Experimental condition LDH FCD/% API/% Reference
SRV-1 fretting friction experiment，run time 60 min，vibration frequency 25 Hz，load 150 N，dosage 0.1%(mass fraction) Co-Al-CO3
Co-Al-Cl
Co-Al-NO3
Co-Al-Ace
Co-Al-DS		 AF*=0.140
AF=0.117
AF=0.103
AF=0.122
AF=0.105		 WV*=33×104 μm3
WV=23×104 μm3
WV=2.5×104 μm3
WV=27×104 μm3
WV=2.5×104 μm3		 [32]
Four ball test, rotary speed 1200 r/min, load 147 N, run time 60 min, dosage 0.25%(mass fraction) Mg-Al-CO3
Mg-Al-Cl		 PB=549 N
PB=598 N		 25.4
37.7		 [46]
Ball disc test, run time 30 min, frequency 25 Hz, load 200 N, dosage 1%(mass fraction) Ni-Al-CO3
Ni-Al-DBP
Ni-Al-OBP		 Third
Second
First		 WV=300×104 μm3
WV=4.2×104 μm3
WV=3.4×104 μm3		 [33]
Four ball test, rotary speed 1200 r/min, load 392 N, run time 60 min, dosage 5 g/L Mg-Al/Ce-CO3
Mg-Al/Ce-LA
Mg-Al/Ce-SA		 27.2
44.7
27.2		 15.9
30.2
16.7		 [29]
Four ball test, rotary speed 1200 r/min，load 392 N, run time 60 min，dosage 5 g/L Mg-Al/La-CO3
Mg-Al/La-SDS		 16.2
26.1		 12.9
16.5		 [47]
Four ball test，rotary speed 1200 r/min，load 392 N, run time 60 min，dosage 10 g/L Co-Al-CO3
Co-Al-SDS		 49.1
50.7		 33.1
17.9		 [39]
Four ball test，rotary speed 1200 r/min，load 392 N，run time 60 min，dosage 10 g/L Mg-Al/Ce-CO3
Mg-Al/Ce-SDS
Mg-Al/Ce-SDSO		 45.15
34.5
20.89		 31.6
16.9
5.1		 [37]
Four ball test，rotary speed 1200 r/min，load 392 N, run time 60 min，dosage 5 g/L Ni-Al-NO3
Ni-Al-LA		 17.3
9.6		 14.7
21.2		 [30]
Table 3  不同阴离子水滑石减摩抗磨性能
LDH Preparation method Crystallization situation FCD/% API/% Reference
Mg-Al/Ce-CO3 Nucleation and
crystallization isolation		 First
Second
Third		 45.15
33.02
35.98		 31.6
18.8
18.6		 [37]
Ni-Al-Cl Microemulsion Width 19.42 nm, thick
8.59 nm		 ≈10 [34]
Mg-Al-CO3 Hydrothermal synthesis Average particle size 350 nm 31.4 30.3 [36]
Co-Al-CO3 Hydrothermal synthesis Crystallinity 92.8%,
particle size 150-200 nm		 49.1 33.1 [39]
Ni-Al-NO3 Coprecipitation Low crystallinity(XRD result)
particle size 40-60 nm		 17.3 14.69 [27]
Mg-Al-NO3 Coprecipitation Low crystallinity(XRD result)
particle size 50-70 nm		 14.4 1.73 [38]
Table 4  水滑石结晶度对减摩抗磨的影响
Fig.1  水滑石减摩抗磨机理示意图
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